2002 03
简论农药残留量检测中的样品前处理技术
基金项目(Foundation):
邮箱(Email):
DOI:
中文作者单位:
中国计量学院生命科学学院 浙江杭州310034
摘要(Abstract):
简要介绍了农药残留量测定中样品的提取、净化等前处理技术最新研究进展 ,包括固相萃取、固相微萃取、超临界流体萃取、微波辅助提取、免疫亲和色谱和凝胶色谱等技术
关键词(KeyWords):
农药残留量;;农药残留量检测;;样品前处理
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参考文献
[1] 姜书会,徐会君.固相萃取技术在农药分析中的应用[J].农业与技术,1999,19(6):35-37.
[2] ARTHUR C L ,PAWL ISZYN J.Solid- phase microextraction with thermal desorption using fused silica opti-cal fibers[J].Anal.Chem.,1990,62:2145.
[3] ARTHUR C L,KILLAM L M,BUCHDZK D,etal.Automation and optimization ofsolid- phased microextraction[J].AnalChem,1992,64:1960.
[4] POPP P,KALBITZ K.Applicaton of solid- phase microextraction and gas chromatography with electron-capture and mass spectrometric detection for the determination of hexachlorocychohexanes in soil solutions[J].JChromatogrA,1994,687:133.
[5] EISERT R,L EVSEN K,WUNSCH G.Element- selective detection of pesticides by gas chromatography-atomic emission detection and solid- phase microextraction[J].JChromatogrA,1994,683:175
[6] ZHANG Z,YANG M J,PAWL ISZYN J.Solid- phase microextraction,a solvent- free alternative for samplepreparation[J].Anal.Chem.,1994,66(17):844A-853A.
[7] CHEN J,PAWLISZYN J.Solid phase microextraction coupled to high- performance liquid chromatography[J].AnalChem,1995,67(15):2530-2533.
[8] 耿昱,郭寅龙.固相微萃取/气相色谱/质谱联用技术在农药残留物分析中的应用[J].分析测试技术与仪器,2001,7(4):230-235.
[9] JINNO K,MURAMATSU T,SAITO Y,et al.Analysis of pesticides in environmental water samples bysolid- phase microextration- high- performance liquid chromatography[J].JChromatogrA,1996,754(1-2):127-135.
[10] 关碧晖,李攻科.SPME-色谱联用技术分析环境样品中除草剂的研究[D].广州:中山大学,2001.
[11] 徐宝才,岳永德,花日茂.超临界流体萃取技术在农药残留分析上的应用[J].安徽农业大学学报,1999,26(2):162-166.
[12] 李萍.氨基甲酸酯农药残留分析方法[J].国外医学-卫生学分册,1999,26(6):366-370.
[13] KREUZIG R,KOINECKE K,BAHADIR M.Use of supercritical fluid extraction in the analysis of pesti-cides in soil[J].Jof biochemical and biophysical methods,2000,43(1-3):403-409.
[14] LOPEZ-AVILA V,YOUNG R,BECKERT W F,et al. microwave- assisted extraction of organic com-pounds from standard reference soils and sediments[J].AnalChem,1994,66:1097-1106.
[15] 冯秀琼,汤庆勇.中草药中14种有机磷农药残留量同时测定——微波辅助提取法[J].农药学报,2001,3(3):45-52.
[16] 高立勤,左文坚.免疫亲和色谱及其在生物样本分析中的应用[J].国外医学药学分册,2000,27(2):107-111.
[17] 李洪波,王绪卿.凝胶渗透色谱净化技术在含油食物农药残留分析中的应用[J].国外医学卫生学分册,1991,1:22-24
[2] ARTHUR C L ,PAWL ISZYN J.Solid- phase microextraction with thermal desorption using fused silica opti-cal fibers[J].Anal.Chem.,1990,62:2145.
[3] ARTHUR C L,KILLAM L M,BUCHDZK D,etal.Automation and optimization ofsolid- phased microextraction[J].AnalChem,1992,64:1960.
[4] POPP P,KALBITZ K.Applicaton of solid- phase microextraction and gas chromatography with electron-capture and mass spectrometric detection for the determination of hexachlorocychohexanes in soil solutions[J].JChromatogrA,1994,687:133.
[5] EISERT R,L EVSEN K,WUNSCH G.Element- selective detection of pesticides by gas chromatography-atomic emission detection and solid- phase microextraction[J].JChromatogrA,1994,683:175
[6] ZHANG Z,YANG M J,PAWL ISZYN J.Solid- phase microextraction,a solvent- free alternative for samplepreparation[J].Anal.Chem.,1994,66(17):844A-853A.
[7] CHEN J,PAWLISZYN J.Solid phase microextraction coupled to high- performance liquid chromatography[J].AnalChem,1995,67(15):2530-2533.
[8] 耿昱,郭寅龙.固相微萃取/气相色谱/质谱联用技术在农药残留物分析中的应用[J].分析测试技术与仪器,2001,7(4):230-235.
[9] JINNO K,MURAMATSU T,SAITO Y,et al.Analysis of pesticides in environmental water samples bysolid- phase microextration- high- performance liquid chromatography[J].JChromatogrA,1996,754(1-2):127-135.
[10] 关碧晖,李攻科.SPME-色谱联用技术分析环境样品中除草剂的研究[D].广州:中山大学,2001.
[11] 徐宝才,岳永德,花日茂.超临界流体萃取技术在农药残留分析上的应用[J].安徽农业大学学报,1999,26(2):162-166.
[12] 李萍.氨基甲酸酯农药残留分析方法[J].国外医学-卫生学分册,1999,26(6):366-370.
[13] KREUZIG R,KOINECKE K,BAHADIR M.Use of supercritical fluid extraction in the analysis of pesti-cides in soil[J].Jof biochemical and biophysical methods,2000,43(1-3):403-409.
[14] LOPEZ-AVILA V,YOUNG R,BECKERT W F,et al. microwave- assisted extraction of organic com-pounds from standard reference soils and sediments[J].AnalChem,1994,66:1097-1106.
[15] 冯秀琼,汤庆勇.中草药中14种有机磷农药残留量同时测定——微波辅助提取法[J].农药学报,2001,3(3):45-52.
[16] 高立勤,左文坚.免疫亲和色谱及其在生物样本分析中的应用[J].国外医学药学分册,2000,27(2):107-111.
[17] 李洪波,王绪卿.凝胶渗透色谱净化技术在含油食物农药残留分析中的应用[J].国外医学卫生学分册,1991,1:22-24
基本信息:
DOI：
中图分类号:S481.8
引用信息:
[1]陈华才.简论农药残留量检测中的样品前处理技术[J].中国计量学院学报,2002(03).
基金信息:
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